气相色谱法分析发酵生物气成分及含量的研究

doi:10.19640/j.cnki.jtau.2018.02.015

Journal of Tianjin Agricultural University ›› 2018, Vol. 25 ›› Issue (2): 60-63.doi: 10.19640/j.cnki.jtau.2018.02.015

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Application of gas chromatography in analysis of fermentation biogenic gas composition and content

YE Tian-yi, LIU Xin-yuan^{Corresponding Author}, NIE Jia-min, YANG Jie, HAN Ze-yu

College of Engineering and Technology, Tianjin Agricultural University, Tianjin 300384, China

Received:2017-11-17 Online:2018-06-20 Published:2019-11-12

Abstract

Abstract: Fermentation biogenic gas is generally composed of several renewable energy gases with complex and changeable composition. A method for determination of hydrogen, nitrogen, methane and carbon dioxide simultaneously in fermentation biogenic gas was established by gas chromatography in this study. The chromatographic peaks were identified efficiently. The standard curves were well fitted in their linear ranges and the component analysis method was capable of very high precision and accuracy. This method was applied in the component analysis of the produced gas in two-stage hydrogen-methane fermentation process for treating food waste, and the way of main composition of fermentation gas change in batch experiment was achieved.

Key words: fermentation biogenic gas, gas chromatography, component analysis, thermal conductivity detector

CLC Number:

S216.4

YE Tian-yi, LIU Xin-yuan, NIE Jia-min, YANG Jie, HAN Ze-yu. Application of gas chromatography in analysis of fermentation biogenic gas composition and content[J]. Journal of Tianjin Agricultural University, 2018, 25(2): 60-63.

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References

[1] 张宝芝,李华锋,翟军峰. 开发生物质能源实现可持续发展[J]. 农业科技与信息,2008(22):10–11.
[2] 岑承志,陈砺,严宗诚,等. 沼气发酵技术发展及应用现状[J]. 广东化工,2009,36(6):78-79,257.
[3] 王勇,任连海,赵冰,等. 初始pH和温度对餐厨垃圾厌氧发酵制氢的影响[J]. 环境工程学报,2017,11(12):6470-6476.
[4] 刘丹. 餐厨废弃物厌氧发酵特性研究[D]. 哈尔滨:东北农业大学,2014.
[5] 黎良新. 大中型沼气工程的沼气净化技术研究[D]. 南宁:广西大学,2007.
[6] 赵光. 两段式厌氧工艺产甲烷发酵特性及微生物生态调控机制研究[D]. 哈尔滨:哈尔滨工业大学,2013.
[7] Lee Y,Chung J.Bioproduction of hydrogen from food waste by pilot-scale combined hydrogen/methane fermentation[J]. International Journal of Hydrogen Energy,2010,35(21):11746-11755.
[8] 于泽. 厌氧接触发酵制氢系统的运行调控与产氢特性[D]. 哈尔滨:哈尔滨工业大学,2012.
[9] 周晓臣. 城镇有机垃圾厌氧发酵中有机酸及氨氮抑制效应研究[D]. 重庆:重庆大学,2006.
[10] 张琪,张继龙,王会刚,等. 气相色谱外标法测定生物柴油中的酯类组分[J]. 现代化工,2013,33(8):134-138.
[11] 李晶宇,张影微,李文哲,等. 气相色谱法测定沼气气体成分及含量的研究[J]. 农机化研究,2015,37(6):255-257.
[12] Krishnan S,Singh L,Sakinah M,et al.Effect of organic loading rate on hydrogen (H₂) and methane (CH₄) production in two-stage fermentation under thermophilic conditions using palm oil mill effluent(POME)[J]. Energy for Sustainable Development,2016,34:130-138.
[13] 刘新媛,鲍振博,彭锦星,等. 餐厨垃圾厌氧发酵制氢技术的研究进展[J]. 天津农学院学报,2017,24(2):95-99.
[14] 杨家添,陈渊. 气相色谱仪热导检测器的使用、调试及灵敏度的测定[J]. 玉林师范学院学报,2001(3):91-92.
[15] 贾斌,靳登超,鲍振博,等. 沼气净化中脱硫技术的研究进展[J]. 天津农学院学报,2016,23(2):57-59,69.

Application of gas chromatography in analysis of fermentation biogenic gas composition and content

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