天津农学院学报 ›› 2024, Vol. 31 ›› Issue (5): 32-39.doi: 10.19640/j.cnki.jtau.2024.05.005

• 研究与简报 • 上一篇    下一篇

基于HS-SPME-GC-MS和PCA分析野生红豆越橘与苹果汁最佳混酿比例的研究

陈瑞, 杨梅, 蒋成, 李默菲, 解冰祎, 张军通信作者   

  1. 天津农学院 食品科学与生物工程学院,天津 300392
  • 收稿日期:2023-07-04 出版日期:2024-10-31 发布日期:2024-11-05
  • 通讯作者: 张军(1980—),男,正高级工程师,博士,研究方向:现代酿造技术及产品开发。E-mail:zjaiwa@163.com。
  • 作者简介:陈瑞(1998—),男,硕士在读,研究方向:食品加工与安全。E-mail:1092267318@qq.com。
  • 基金资助:
    天津市技术创新引导专项(21YDTPJC00910); 中央引导地方科技发展专项(21ZYCGSN00410); 天津市科技成果转移转化项目(22ZYCGSN00060)

Research on optimal blending ratio of wild red bean lingonberry and apple juice based on HS-SPME-GC-MS and PCA analysis

Chen Rui, Yang Mei, Jiang Cheng, Li Mofei, Xie Bingyi, Zhang JunCorresponding Author   

  1. College of Food Science and Bioengineering, Tianjin Agricultural University, Tianjin 300392, China
  • Received:2023-07-04 Online:2024-10-31 Published:2024-11-05

摘要: 以野生红豆越橘和苹果汁为原料,研究两者不同混酿比例对野生红豆越橘混酿果酒理化指标、香气成分和感官特性的影响。采用顶空固相微萃取-气质联用(HS-SPME-GC-MS)和主成分分析(PCA)方法对不同混酿比例的野生红豆越橘果酒进行香气成分分析。结果表明:9种样品中共检测出154种香气成分,其中共有成分17种,醇类、酯类是野生红豆越橘果酒香气的重要组成部分。主成分分析结果显示,9种样品中共提取出8个主成分,其中第一主成分共45种,贡献率为36.935%,第一主成分包括大马士酮、癸酸、苯乙酮等。感官评价结果显示,野生红豆越橘与苹果汁体积比例为4∶6的酒样感官评分最高,为90分,酒体口感清爽,醇香浓郁,典型性强。由此可知,野生红豆越橘与苹果汁体积比为4∶6的酒样能完全发酵,野生红豆越橘与苹果果香平衡协调,其他比例混酿果酒醇类或酸类较高,香气复杂,口感粗糙。

关键词: 野生红豆越橘, 苹果汁, 混酿, HS-SPME-GC-MS, PCA

Abstract: Using wild red bean lingonberry and apple juice as raw materials, the effects of different blending ratios on the physical and chemical indicators, aroma components and sensory characteristics of wild red bean lingonberry blended fruit wine were studied. Headspace solid-phase microextraction-gas chromatography-mass spectrometry(HS-SPME-GC-MS)and principal component analysis(PCA)were used to analyze the aroma components of wild red bean lingonberry fruit wine with different blending ratios. The results showed that a total of 154 aroma components were detected in 9 samples, of which 17 were shared conponent. Alcohols and esters were important components of the aroma of wild red bean lingonberry fruit wine. The results of principal component analysis showed that a total of 8 principal components were extracted from 9 samples, of which 45 were the first principal components, with a contribution rate of 36.935%. The first principal components included damascenone, capric acid, acetophenone, etc. The sensory evaluation results showed that the wine sample with a volume ratio of 4∶6 of wild red bean lingonberry and apple juice had the highest sensory score of 90 points. Conclusion: The wine sample with a volume ratio of 4∶6 of wild red bean lingonberry and apple juice can be completely fermented, and the fruit aroma of wild red bean lingonberry and apple is balanced and coordinated, while other ratios of blended fruit wine have higher alcohols or acids, with complex aroma and rough taste.

Key words: wild red bean lingonberry, apple juice, blended wine, HS-SPME-GC-MS, PCA

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