环境样品中抗生素的前处理及检测方法研究进展

Journal of Tianjin Agricultural University ›› 2017, Vol. 24 ›› Issue (3): 92-96.

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Pretreatment and Detection Methods of Antibiotics in Environmental Samples

JIN Lu^1a, CHEN Pin-pin^1a, WANG Xiao^1a, ZHAO Yu-kun^1a, LI De-kang^1a, JI Xin-ning^1b, WU Nan^{1a,Corresponding Author}

1. Tianjin Agricultural University, a. College of Engineering and Technology, b. College of Horticulture and Landscape, Tianjin 300384, China

Online:2017-09-30 Published:2019-10-15

Abstract

Abstract: The environmental problems caused by the extensive use of antibiotics are becoming increasingly serious, and it is urgent to establish effective methods for antibiotics analysis. However, due to the complex compositions of environmental samples and trace levels of antibiotics, the samples usually need to go through the complex extraction, purification, concentration and other pretreatment processes before analysis. The principles, applications, advantages and disadvantages of various pretreatment and detection methods of antibiotics in environmental samples are systematically elaborated and future prospects are proposed as well.

Key words: environmental samples, antibiotics, pretreatment methods, detection methods

CLC Number:

JIN Lu, CHEN Pin-pin, WANG Xiao, ZHAO Yu-kun, LI De-kang, JI Xin-ning, WU Nan. Pretreatment and Detection Methods of Antibiotics in Environmental Samples[J]. Journal of Tianjin Agricultural University, 2017, 24(3): 92-96.

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References

[1] 吴楠,杨静慧,张伟玉,等. 不同环境介质中抗生素耐药性的检测方法研究进展[J]. 微生物学通报,2016,43(12):2720-2729.
[2] 马丽丽,郭昌胜,胡伟,等. 固相萃取-高效液相色谱-串联质谱法同时测定土壤中氟喹诺酮、四环素和磺胺类抗生素[J]. 分析化学,2010,38(1):21-26.
[3] 赵健,杨晓凡,周福来,等. 固相萃取/高效液相色谱/串联质谱法测定磺胺类抗生素[J]. 中国给水排水,2012,28(14):107-110.
[4] Li B,Zhang T,Xu Z,et al.Rapid analysis of 21 antibiotics of multiple classes in municipal wastewater using ultra performance liquid chromatography-tandem mass spectrometry[J]. Analytica Chimica Acta,2009,645(1/2):64-72.
[5] 孙刚. 畜禽粪便中四环素类抗生素检测分析及其在堆肥中的降解研究[D]. 合肥:合肥工业大学,2010.
[6] 彭贵龙,何强,周光明,等. 微萃取/高效液相色谱法测定污泥中的抗生素TAP、FF[J]. 中国给水排水,2015,31(20):112-116.
[7] 庄园,彭英,赵永刚,等. 分子印迹固相微萃取-高效液相色谱法测定水和牛奶中三种四环素类药物[J]. 分析科学学报,2014,30(4):451-456.
[8] 周爱霞,苏小四,高松,等. 高效液相色谱测定地下水、土壤及粪便中4种磺胺类抗生素[J]. 分析化学,2014,42(3):397-402.
[9] 孙宝利,袁志华,申秀丽,等. ASE-HPLC-MS/MS法测定土壤中四环素类抗生素残留[J]. 农业资源与环境学报,2013,30(1):79-82.
[10] 唐才明,黄秋鑫,余以义,等. 污泥和沉积物中微量大环内酯类、磺胺类抗生素、甲氧苄胺嘧啶和氯霉素的测定[J]. 分析化学,2009,37(8):1119-1124.
[11] 孙奉翠. 土壤中四类典型抗生素的同时测定及其方法优化[D]. 济南:山东大学,2013.
[12] 胡献刚. 环境中典型抗生素测定方法、污染水平与归宿[D]. 天津:南开大学,2009.
[13] 国明,于峰,贾科玲,等. 磁性固相萃取-高效液相色谱-串联质谱法测定环境水样中的四环素类抗生素[J]. 色谱,2016,34(4):407-413.
[14] 李明月,孙倩,王琴,等. 污泥中典型抗生素的检测[J]. 环境工程学报,2016,10(2):985-991.
[15] 杨晓蕾,李杰,李学文,等. 土壤中10种兽用抗生素的固相萃取-高效液相色谱-紫外测定法[J]. 环境与健康杂志,2012,29(4):357-360.
[16] 贺南南,管永祥,梁永红,等. 高效液相色谱-荧光检测法同时分析沼液中4种喹诺酮类抗生素[J]. 农业环境科学学报,2016,35(10):2034-2040.
[17] 戴晓虎,薛勇刚,刘杰华,等. 基于固相萃取及高效液相色谱-荧光检测分析的污泥中氟喹诺酮类抗生素研究方法的开发[J]. 环境科学,2016,37(4): 1553-1561.
[18] 邰义萍,莫测辉,李彦文,等. 广州市某绿色和有机蔬菜基地土壤中四环素类抗生素的含量与分布特征[J]. 农业环境科学学报,2014,33(9):1743-1748.
[19] Pan X,Qiang Z,Ben W,et al.Residual veterinary antibiotics in swine manure from concentrated animal feeding operations in Shandong Province,China[J]. Chemosphere,2011,84(5):695-700.
[20] Ho Y B,Zakaria M P,Latif P A,et al.Simultaneous determination of veterinary antibiotics and hormone in broiler manure,soil and manure compost by liquid chromatography-tandem mass spectrometry[J]. Journal of Chromatography A,2012,1262(21):160-168.
[21] Zhu J,Snow D D,Cassada D A,et al.Analysis of oxytetracycline,tetracycline,and chlortetracycline in water using solid-phase extraction and liquid chromatography- tandem mass spectrometry[J]. Journal of Chromatography A,2001,928(2):177-186.
[22] Zhou L J,Ying G G,Liu S,et al.Simultaneous determination of human and veterinary antibiotics in various environmental matrices by rapid resolution liquid chromatography-electrospray ionization tandem mass spectrometry[J]. Journal of Chromatography A,2012,1244(12):123-138.
[23] 吴晓凤,郑嘉熹,魏源送,等. 超高效液相色谱串联质谱法同时检测复杂基质中四环素类抗生素及其代谢产物[J]. 农业环境科学学报,2013,11(11):2293-2301.
[24] Zheng W L,Zhang L F,Zhang K Y,et al.Determination of tetracyclines and their epimers in agricultural soil fertilized with swine manure by ultra-high-performance liquid chromatography tandem mass spectrometry[J]. Journal of Integrative Agriculture,2012,11(7):1189-1198.

Pretreatment and Detection Methods of Antibiotics in Environmental Samples

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